Production of AA2124/MoSi2/25p composites and effect of heat treatment on their microstructure, hardness and compression properties

Authors

  • Fatemeh Piyadeh Materials and Metallurgical Engineering Department, Semnan University
  • Hassan Abdollah-Pour Materials and Metallurgical Engineering Department, Semnan University
  • Marcela Lieblich Centro Nacional de Investigaciones Metalúrgicas (CENIM-CSIC)

DOI:

https://doi.org/10.3989/revmetalm.030

Keywords:

Aluminium matrix composites, MoSi2 intermetallic reinforcement, Powder metallurgy, Wear properties

Abstract


AA2124/25vol%MoSi2 composites were processed by two powder metallurgy routes: high energy ball milling of the reinforcement and alloy powder (B composite) and wet blending with cyclohexane (W composite), both followed by extrusion to achieve full consolidation. As-extruded and heat treated composite bars were studied microstructurally and mechanically (hardness and compression tests under quasistatic loading). Microstructure and fracture profiles were observed by scanning electron microscopy and the reaction products formed in the matrix were identified by energy-dispersive X-ray spectroscopy and X-ray diffraction analysis. The results show that for both composites, the hardness of the specimens in solution and aged condition was higher than in the as-extruded condition. The hardness of the B composite was higher than that of the W composite whereas the age-hardenability of the B composite was significantly lower than that of the W composite. After heat treatments, small diffusion reaction phases appeared at the interface between matrix and reinforcements. Compressive yield strength and the ultimate strength of both composites improved considerably after the artificial ageing. The composite fracture surfaces exhibited microscopically a ductile appearance that consisted of dimples in the matrix and a fragile fracture of the MoSi2 particulates.

Downloads

Download data is not yet available.

References

Arakawa, S., Hatayama, T., Matsugi, K., Yanagisawa, O. (2000). Effect of heterogeneous precipitation on age hardening of Al2O3 particle dispersion Al–4mass% Cu composite produced by mechanical alloying. Scripta Mater. 42, 755–760. http://dx.doi.org/10.1016/S1359-6462(99)00426-1

ASTM E9-09 (2009). Standard Test Methods of Compression Testing of Metallic Materials at Room Temperature, ASTM International.

Bhanu Prasad, V.V., Bhat, B.V.R., Mahajan, Y. R., Ramakrishnan, P. (2002). Structure–property correlation in discontinuously reinforced aluminium matrix composites as a function of relative particle size ratio. Mater. Sci. Eng. A 337, 179–186. http://dx.doi.org/10.1016/S0921-5093(02)00024-2

Chawla, N., Chawla, K.K. (2006). Metal Matrix Composites. Ed. Springer.

Clyne, T.W., Withers, P.T. (1993). An Introduction to Metal Matrix Composites. Ed. Cambridge University Press.

Corrochano, J., Lieblich, M., Ibá-ez, J. (2009). On the role of matrix grain size and particulate reinforcement on the hardness of powder metallurgy Al–Mg–Si/MoSi2 composites. Composites Sci. Tech. 69, 1818–1824. http://dx.doi.org/10.1016/j.compscitech.2009.03.017

Corrochano, J., Walker, J.C., Lieblich, M., Ibá-ez, J., Rainforth, W.M. (2011). Dry sliding wear behaviour of powder metallurgy Al-Mg-Si alloy-MoSi2 composites and the relationship with the microstructure. Wear 270, 658–665. http://dx.doi.org/10.1016/j.wear.2011.01.029

González-Carrasco, J. L., García Cano, F., Carauna, J., Lieblich, M. (1994). Aluminium/Ni3Al composites processed by powder metallurgy. Mater. Sci. Eng. A 183, L5–L8. http://dx.doi.org/10.1016/0921-5093(94)90914-8

Kang, Y.C., Chan, S.L.I. (2004). Tensile properties of nanometric Al2O3 particulate reinforced aluminum matrix composites. Mater. Chem. Phys. 85, 438–443. http://dx.doi.org/10.1016/j.matchemphys.2004.02.002

Khakbiz, M., Akhlaghi, F. (2009). Synthesis and structural characterization of Al–B4C nano-composite powders by mechanical alloying. J. Alloys Compd. 479, 334–341. http://dx.doi.org/10.1016/j.jallcom.2008.12.076

Lieblich, M., González-Carrasco, J.L., Caruana, G. (1997). Thermal stability of an Al/Ni3Al composite processed by powder metallurgy. Intermetallics 5, 515–524. http://dx.doi.org/10.1016/S0966-9795(97)00027-7

Lu, L., Lai, M.O., Ng, C.W. (1998). Enhanced mechanical properties of an Al based metal matrix composite prepared using mechanical alloying. Mater. Sci. Eng. A 252, 203–211. http://dx.doi.org/10.1016/S0921-5093(98)00676-5

Merle, P. (2000). Thermal treatments of age-hardenable metal matrix composites. MMC-Assess Thematic Network, Vol 2, pp. 1–24. Available on line: http://mmc-assess.tuwien.ac.at/public/v2_thermaltreat.pdf

Omura, H., Miyoshi, T., Takahashi, Y., Conley, C.G., Yodogawa, M. (1988). Dispersion Strengthened Aluminum Alloys, Y.-M. Kim and W.M. Griffith (Eds.). The Minerals, Metals, and Materials Society, Warrendale, PA, p. 421.

Parvin, N., Assadifard, R., Safarzadeh, P., Sheibani, S., Marashi, P. (2008). Preparation and mechanical properties of SiC-reinforced Al6061 composite by mechanical alloying. Mater. Sci. Eng. A 492, 134–140. http://dx.doi.org/10.1016/j.msea.2008.05.004

Pour, H.A., Lieblich, M., López, A.J., Rams, J., Salehi, M.T., Shabestari, S.G. (2007). Assessment of tensile behaviour of an Al–Mg alloy composite reinforced with NiAl and oxidized NiAl powder particles helped by nanoindentation. Composites Part A: Applied Science and Manufacturing 38 (12), 2536–2540. http://dx.doi.org/10.1016/j.compositesa.2007.07.012

Sameezadeh, M., Emamy, H., Farhangi, H. (2010). Effects of particulate reinforcement and heat treatment on the hardness and wear properties of AA 2024-MoSi2 nanocomposites. Mater. Des. 32 (4), 2157–2164. http://dx.doi.org/10.1016/j.matdes.2010.11.037

Silva-Maia, P.B., Velasco, F., Zapata, W.C., Torralba, J.M. (1999). Intergranular corrosion resistance of 2014 aluminum alloys reinforced with Ni3Al. Mater. Sci. Forum 299, 279–285. http://dx.doi.org/10.4028/www.scientific.net/MSF.299-300.279

Smith, G.W. (1998). Precipitation kinetics in solutionized aluminum alloy 2124: Determination by scanning and isothermal calorimetry. Thermochemical Acta 317, 7–23. http://dx.doi.org/10.1016/S0040-6031(98)00361-X

Suryanarayana, C. (2001). Mechanical alloying and milling. Prog. Mater. Sci. 46, 1–184. http://dx.doi.org/10.1016/S0079-6425(99)00010-9

Tanaka, K., Nawata, K., Inue, H., Yamaguchi, M., Koiwa, M. (2001). Refinement of crystallographic parameters in transition metal disilisides with the C11b, C40 and C45structures. Intermetallic 9, 603–607. http://dx.doi.org/10.1016/S0966-9795(01)00048-6

Torres, B., Lieblich, M., Ibá-ez, J., García-Escorial, A. (2002). Mechanical properties of some PM aluminide and silicide reinforced 2124 aluminium matrix composites. Scripta Mater. 47, 45–49. http://dx.doi.org/10.1016/S1359-6462(02)00095-7

Walker, J.C., Rainforth, W.M., Jones, H. (2005). Lubricated sliding wear behavior of aluminium alloy composites. Wear 259, 577–589. http://dx.doi.org/10.1016/j.wear.2005.01.001

Zhou, J., Duszczyk, J., Korevaar, B.M. (1990). The relationship between extrusion conditions and tensile properties of a P/M Al-Fe-Si-Fe-Cu-Mg alloy with a high volume fraction of intermetallic compounds. Proceeding of World Conference on Powder Metallurgy, Vol. 8. Institute of Metals, P. 307, London, pp. 91–100.

Published

2014-12-30

How to Cite

Piyadeh, F., Abdollah-Pour, H., & Lieblich, M. (2014). Production of AA2124/MoSi2/25p composites and effect of heat treatment on their microstructure, hardness and compression properties. Revista De Metalurgia, 50(4), e030. https://doi.org/10.3989/revmetalm.030

Issue

Section

Articles

Most read articles by the same author(s)