Microstructural and mechanical evolution of AA6063/SiC/WC composites under aging and rolling conditions
DOI:
https://doi.org/10.3989/revmetalm.e270.1675Keywords:
AA6063/SiC/WC, Aging, Mechanical properties, Rheo stir casting, Rolling, Scanning Electron MicroscopeAbstract
This work seeks to enhance the rheo-stir casting method for the fabrication of an aluminium alloy 6063-based metal matrix composite, reinforced with silicon carbide (SiC) and tungsten carbide (WC) in different weight proportions—SiC from 2% to 6% and WC from 0.2% to 1%. Subsequent investigation was conducted on the AA6063 composite reinforced with 4% SiC and 0.6% WC, examining the effects of varying processing parameters during solution heat treatment and rolling on the material's characteristics. Microstructural investigation demonstrated that the incorporation of SiC and WC particles into the AA6063 matrix induced a pinning effect, resulting in a refinement of the grain structure through a reduction in grain size. With the augmentation of SiC and WC proportions, the composite demonstrated enhanced mechanical capabilities. The sample with 6% SiC and 1% WC attained the maximum microhardness (110 Hv), ultimate tensile strength (215 MPa), and yield strength (146 MPa), enhancements ascribed to the strengthening impact from the uniform distribution of the reinforcements. The rheo-stir casting method markedly improved the compaction and uniform dispersion of reinforcing particles in the AA6063/SiC/WC composites. Hardness increased due to precipitation hardening, resulting from the dissolution of secondary phases during homogenization. The specimen subjected to cryo-rolling achieved the maximum hardness of 170 Hv among all rolling techniques, despite an 80% loss in thickness, due to the inhibition of dynamic recovery. The experimentally obtained yield strength exceeded the projected theoretical value when accounting for the impacts of multiple strengthening mechanisms.
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Alcántara Alza, V. (2021). Effect of Aging and Deformation Treatments on Mechanical Properties of Aluminum AA-6063. Recent Technology and Engineering (IJRTE) 9 (6), 158-167. https://doi.org/10.35940/ijrte.F5532.039621
Dejun, K., Chengjian, T. (2017). Effects of Loads on High-Temperature Friction-Wear Properties of Cathodic Arc Ion Plated TiALSiN Coatings. Surf. Rev. Lett. 24 (Supp 02), 1850034. https://doi.org/10.1142/S0218625X18500348
Etesami, S.A., Fotovvati, B., Asadi, E. (2022). Heat treatment of Ti-6Al-4V alloy manufactured by laser-based powder-bed fusion: Process, microstructures, and mechanical properties correlations. J. Alloys Compd. 895 (Part 2), 162618. https://doi.org/10.1016/j.jallcom.2021.162618
Granum, H., Myhr, O.R., Børvik, T., Hopperstad, O.S. (2021). Effect of pre-stretching on the mechanical behaviour of three artificially aged 6xxx series aluminium alloys. Mater. Today Commun. 27, 102408. https://doi.org/10.1016/j.mtcomm.2021.102408
Grilo, J., Carneiro, V.H., Teixeira, J.C., Puga, H. (2021). Manufacturing methodology on casting-based aluminium matrix composites: Systematic Review. Metals 11 (3), 436. https://doi.org/10.3390/met11030436
Jeevansuriya, R., Sridhar, R., Pugazhenthi, R. (2024). Study the mechanical and morphological properties of aluminium alloy 7075 by aging treatments. Mater. Today Proc. https://doi.org/10.1016/j.matpr.2024.06.008
Jiang, J., Cui, J., Wang, Y., Huang, M., Dong, J., Yan, J. (2024). Effect of T6 heat treatment on microstructure and mechanical properties of 6082 aluminum alloy automotive flange components formed by squeeze casting. Mater. Sci. Eng. A 912, 146974. https://doi.org/10.1016/j.msea.2024.146974
Kandpal, B.C., Kumar, J., Singh, H. (2018). Manufacturing and technological challenges in Stir casting of metal matrix composites-A Review. Mater. Today Proc. 5 (1), 5-10. https://doi.org/10.1016/j.matpr.2017.11.046
Li, G., Ruan, G., Huang, Y., Xu, Z., Li, X., Guo, C., Zhao, C, Cheng, L., Hu, X., Li, X., Zhu, Q. (2022). Facile and cost-effective approach to additively manufacture crack-free 7075 aluminum alloy by laser powder bed fusion. J. Alloys Compd. 928, 167097. https://doi.org/10.1016/j.jallcom.2022.167097
Li, W., Wu, M., Xiao, D., Huang, L., Liu, W., Tang, S. (2022). Effect of Rolling Temperature on Microstructure and Properties of Al-Mg-Li Alloy. Materials 15 (21), 7517. https://doi.org/10.3390/ma15217517 PMid:36363108 PMCid:PMC9656105
Mao, H., Shen, F., Zhang, Y., Wang, J., Cui, K., Wang, H., Tan, T. (2021). Microstructure and mechanical properties of carbide reinforced TiC-based ultra-high temperature ceramics: A Review. Coatings 11 (12), 1444. https://doi.org/10.3390/coatings11121444
Olorunyolemi, O.C., Ogunsanya, O.A., Akinwande, A A., Balogun, O.A., Saravana Kumar, M. (2022). Enhanced mechanical behaviour and grain characteristics of aluminium matrix composites by cold rolling and reinforcement addition (Rice husk ash and Coal fly ash). P. I. ENG. E-J. PRO. https://doi.org/10.1177/09544089221124462
Pant, R., Joshi, K., Singh, A., Joshi, K., Gupta, A. (2024). Mechanical properties evaluation of ultra fined grained materials at low temperature. AIP Conf. Proc. 2978 (1), 020008. https://doi.org/10.1063/5.0189994
Ramachandran, K.K., Murugan, N., Kumar, S.S. (2015). Effect of tool axis offset and geometry of tool pin profile on the characteristics of friction stir welded dissimilar joints of aluminum alloy AA5052 and HSLA steel. Mater. Sci. Eng. A 639, 219-233. https://doi.org/10.1016/j.msea.2015.04.089
Rao, P.N., Singh, D., Brokmeier, H.G., Jayaganthan, R. (2015). Effect of ageing on tensile behavior of ultrafine grained Al 6061 alloy. Mater. Sci. Eng. A 641, 391-401. https://doi.org/10.1016/j.msea.2015.06.036
Saravanan, R., Krishnan, P.B. (2014). Effect on post weld heat treatment process in different aluminium alloys 6063 and 319. In Second International Conference on Current Trends in Engineering and Technology-ICCTET 2014, pp. 74-77. https://doi.org/10.1109/ICCTET.2014.6966265
Singh, L., Kumar, S., Raj, S., Shivam, Badhani, P. (2021). Development and characterization of aluminium silicon carbide composite materials with improved properties. Mater. Today Proc. 46 (Part 15), 6733-6736. https://doi.org/10.1016/j.matpr.2021.04.220
Singh, N.K., Balaguru, S. (2024). Fabrication and mechanical characterization of Al-Zn-Cu Alloy/SiC/TiB2 hybrid reinforced metal matrix composite using top loaded bottom pouring stir casting method. Silicon 16 (1), 45-59. https://doi.org/10.1007/s12633-023-02648-4
Wu, Z.-H., Mao, Q.-J., Hua, F.-A., Jia, G.-L., Li, J.-P., Li, C.-G., Yuan, G., Wang, G.-D. (2022). Researches on the Macro- and Micro-Structures and Properties of the Vertical Bending Continuous Casted AA6063 Thin Slabs and Their As-Rolled Sheets. Metals 12 (11), 1937. https://doi.org/10.3390/met12111937
Xu, G.F., Olorunyolemi, T., Wilson, O.C., Lloyd, I.K., Carmel, Y. (2002). Microwave sintering of high-density, high thermal conductivity AlN. J. Mater. Res. 17 (11), 2837-2845. https://doi.org/10.1557/JMR.2002.0412
Xu, Y., Zhang, Z., Gao, Z., Bai, Y., Zhao, P., Mao, W. (2021). Effect of main elements (Zn, Mg and Cu) on the microstructure, castability and mechanical properties of 7xxx series aluminum alloys with Zr and Sc. Mater. Charact. 182, 111559. https://doi.org/10.1016/j.matchar.2021.111559
Yao, X., Zheng, Y.F., Liang, J.M., Zhang, D.L. (2015). Microstructures and tensile mechanical properties of an ultrafine grained AA6063-5 vol% SiC metal matrix nanocomposite synthesized by powder metallurgy. Mater. Sci. Eng. A 648, 225-234. https://doi.org/10.1016/j.msea.2015.09.059
Zhou, L., Hyer, H., Chang, J., Mehta, A., Huynh, T., Yang, Y., Sohn, Y. (2021). Microstructure, mechanical performance, and corrosion behavior of additively manufactured aluminum alloy 5083 with 0.7 and 1.0 wt% Zr addition. Materials Science and Engineering: A 823, 141679. https://doi.org/10.1016/j.msea.2021.141679
Zhou, Y., Lin, M., Liu, C., Wang, L., Chen, H., Dan, C., Dan, C., Ma, S., Chen, Z., Wang, H. (2022). Enhancing mechanical properties of uniformly distributed nano TiB2/2024 Al composite rolling sheet by pre-stretch aging. J. Alloys Compd. 913, 165172. https://doi.org/10.1016/j.jallcom.2022.165172
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